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Publication Title | United States Patent US7125527

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(12)United States Patent H01]

(54) RMSEUEACTCHTOMODERSTSHOAOFNDODSPREERACTTIONRGSSUERMFPALCOEYING

(75) Inventor: RichardA.H0ll,Camarillo,CA(US)

(73) Assignee: KinetiChem,Inc.,Camarillo,CA(US)

(10)PatentN0.: US 7,125,527B2 (45)Date ofPatent: Oct.24,2006

* Notice: Sub'ecttoan disclaimer,thetermofthis Jy*..

patent is extended or adjusted under 35 U'S'C' 154(1)) by 278 days‘

(21) Appl.N0.:10/656,627

cued by examlner Primary ExamineriN. Bhat

(22) Filed: (65)

Sep.5,2003

Methods of operating surface reactors, and such reactors, particularlyspinningdiscreactorsrequirethata?rstreactant is fed to the reactor surface and forms a thin ?lm on the

surface.A secondreactantisfedtothesurfaceintheform of a second thin ?lm to interact With the ?rst ?lm so as to overcome the impedance to interaction betWeen the tWo ?lms imposed by the existence of molecular clusters in the ?lms. Thus, each ?lm is fed into the receiving ?lm at a rate such as to break up the molecular clusters in the ?lm and therebypermitthemoleculestoaggressivelyandcompletely interact With one another. In the spinning disc apparatus the ?lmsarefedatrespectivedistancesfromthespinaxis.The interaction takes place in a thin chamber (less than 1 mm) betWeen a retaining surface coextensive With the reactor surface Whose distance from one another can be varied continuously, With the components being sheared betWeen the surfaces to break up the molecular clusters to facilitate

200

Pnor Pubhcatlon Data US 2005/0053532A1 Mar.10,2005

(51) Int.Cl. B01] 8/08

(2006.01) (2006.01)

(2006.01)

422/209,422/224,261/86; 261/89

(52) (58)

(56)

B01D 47/16 B01F3/04

us.c1.

FieldofClassi?cationSearch 422/135,

422/138,186, 186.3, 224, 129, 209, 100, 261/86, 89

See application ?le for complete Search history, _

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ABSTRACT

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526/62 2005/0158220 Al* 7/2005 Ramshaw eta1. 422/186

FOREIGNPATENTDOCUMENTS

1464389 * 10/2004 EP 0499362 * 10/2004 2108407 * 5/1983

2004/02346104390 A1* 121/2004 Jachucketa1.

Image | United States Patent US7125527



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