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Publication Title | ENCAPSULATED LABILE COMPOUND COMPOSITIONS AND METHODS OF MAKING THE SAME

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United States Patent Subramanian et a].

ENCAPSULATED LABILE COMPOUND COMPOSITIONS AND METHODS OF MAKING THE SAME

(10) Patent N0.: US 8,221,809 B2 (45) Date of Patent: Jul. 17, 2012

Inventors:

Assignee:

Notice:

Srinivasan Subramanian, Broom?eld, CO (US);BrianJ.Connolly, Broom?eld,CO (US);WilliamA. Hendrickson,StillWater,MN (US)

MartekBiosciencesCorporation, Columbia,MD (US)

Subject to any disclaimer, the term of this patent is extended or adjusted under 35 USC 154(b)by607days.

6,444,227 B1 6,444,242 B1 6,599,556 B2 6,770,104 B2 6,974,592 B2 6,991,823 B2 7,001,610 B2

9/2002 Leuenbergeretal. 9/2002 Skelbaeketa1. 7/2003 Starketa1. 8/2004 Murphy

12/2005 Yan

1/2006 Augustineta1. 2/2006 Stewart 4/2003 Wilsoneta1.

App1.No.:11/767,366

2004/0191390 A1 2005/0019416 A1 2005/0067726 A1 2005/0233002 A1 2005/0238788 A1 2005/0281926 A1 2006/0159805 A1 2006/0286205 A1 2008/0020086 A1 2008/0096964 A1 2009/0004233 A1

9/2004 Lee 1/2005 Yan 3/2005 Yaneta1.

10/2005 Trubiano eta1. 10/2005 Buononato eta1. 12/2005 Yangeta1.

7/2006 Fundaeta1. 12/2006 Fichtalieta1. 1/2008 Abrileta1.

4/2008 Subramanianeta1. 1/2009 Connollyeta1.

Filed:

Jun.22,2007

Prior Publication Data

US 2008/0026108A1

Jan.31,2008

0 249 282 A1 0385081

Related US. Application Data

ProvisionalapplicationNo.60/805,590,?ledonJun. 22, 2006, provisional application No. 60/945,040, ?led on Jun. 19, 2007.

0 387 597 A2 0385081

Int.Cl.

A23B 4/10

US. Cl. .. 426/89; 426/96; 426/98; 426/302 Field of Classi?cation Search ................... 426/89,

426/98 Seeapplication?leforcompletesearchhistory.

3,655,864 A 3,804,776 A 3,819,838 A 4,217,370 A 4,332,790 A 4,533,557 A 4,675,189 A 4,678,710 A 4,895,725 A 4,957,748 A 5,015,483 A 5,106,639 A 5,143,737 A 5,153,177 A 5,190,775 A 5,206,041 A 5,213,810 A 5,356,636 A 5,496,571 A 5,698,244 A 5,756,143 A 5,789,001 A 5,874,470 A 5,908,654 A 5,985,348 A 6,013,286 A 6,083,520 A 6,245,366 B1 6,248,909 B1 6,258,964B1

4/1972 Grass,Jr.eta1. 4/1974 YaZaWaeta1. 6/1974 Smithetal. 8/1980 Rawlingsetal. 6/1982 SoZZieta1. 8/1985 Maruyamaetal. 6/1987 Kenteta1. 7/1987 Sakimotoetal. 1/1990 Kantoretal. 9/1990 Winowiski 5/1991 Haynesetal. 4/1992 Leeeta1. 9/1992 Richardson

10/1992 Chaundyetal. 3/1993 Klose

4/1993 Wellons 5/1993 Steber

10/1994 Schneideretal. 3/1996 Blagdonetal.

12/1997 Barclay

5/1998 Caineta1. 8/1998 Klopfensteineta1. 2/1999 Nehneeta1. 6/1999 Caineta1.

11/1999 Barclay

1/2000 Klose

7/2000 Toneby

6/2001 Popplewelleta1. 6/2001 Akimoto etal. 7/2001 Nakajimaetal.

References Cited U.S.PATENT DOCUMENTS

(Continued)

OTHER PUBLICATIONS

Klinkesorn et al, “Stability of Spray-Dried Tuna Oil Emulsions Encapsulated with Two-Layered Interfacial Membranes”, J. Agric. Food Chem., Sep. 23, 2005*

Lactobacillus acidophilus, http://alternativedr.com/lactobacillusi acidophilus,archiveorgFeb.2006* Gouin,S.Microencapsulation:IndustrialAppraisalofExistingTech nologies and Trends. Food Science and Technology 15 (2004) 330 347. InternationalPreliminaryReportofPatentabilityandWrittenOpin ionforPCT ApplicationNo. PCT/US07/071938,mailedJan.8,2009, 4 pages.

InternationalSearchReportandWrittenOpinionforPCT Applica tion No. PCT/US07/071938, mailed Nov. 13, 2007, 8 pages.

(Continued)

PrimaryExaminer* LienTran

(74)Attorney,Agent,orFirm* Sterne,Kessler,Goldstein & Fox P.L.L.C.

(57) ABSTRACT

Products comprising labile compounds, such as polyunsatu ratedfattyacids,andhaving?rstandsecondencapsulantsare disclosed.A ?rstencapsulantcanbeaspraydriedcoatingand the second encapsulant can be a prill coating. Methods of making the same are provided.

38Claims,1DrawingSheet

(2006.01)

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JP 63-023736 A JP 08-336360 A W0 WO 91/05482 W0 WO92/12711A1 W0 WO95/06414A1

12/1987 5/1990 9/1990 9/1990

11/1994 9/1998 1/2006 9/2006

12/1970 2/1988 12/1996 5/1991 8/1992 3/1995

US008221809B2

2003/0072787 A1

2003/0185960 A1

2003/0193102 A1

2003/0211221 A1* 11/2003 Abrileta1. ...................426/601

10/2003 Augustineta1. 10/2003 Yan

FOREIGN PATENT DOCUMENTS

0 626 172 A1 0 862 369 B1

1616486

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